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Crystal Structures of Dipeptides Derived from the beta-Amino Acids (1R,2S)-2-Aminocyclopentanecarboxylic Acid and (1S,2R,3S)-2-Amino-3-methylcyclopentanecarboxylic Acid

Abstract:

Crystals of the dimeric β-peptides 13 and 20, derived from (1R,2S)-2-aminocyclopentanecarboxylic acid and (1S,2R,3S)-2-amino-3- methylcyclopentanecarboxylic acid, respectively, were synthesised and studied by X-ray diffraction in order to establish their solid state secondary structural characteristics. Compound 13 crystallises in the monoclinic space group P 2 1 with cell parameters of a = 5.2682(1) Å, b = 9.1211(2) Å, c = 22.4467(6) Å, β = 91.3855(9)°, V = 1078.29(4) Å3 and Z = 2. Compound ...

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Publication status:
Published

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Publisher copy:
10.1007/s10870-011-0164-x

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
Volume:
41
Issue:
11
Pages:
1722-1728
Publication date:
2011-11-01
DOI:
EISSN:
1572-8854
ISSN:
1074-1542
Source identifiers:
206197
Language:
English
Keywords:
Pubs id:
pubs:206197
UUID:
uuid:35d0996c-3a6c-4717-811e-bebc35aaa20d
Local pid:
pubs:206197
Deposit date:
2012-12-19

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