Journal article
High energy X-rays for following metal-organic framework formation: identifying intermediates in interpenetrated MOF-5 crystallisation
- Abstract:
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We report a study of the solvothermal formation of the interpenetrated form of the zinc 1,4-benzene dicarboxylate (BDC) metal organic framework MOF-5 using high-energy in situ X-ray diffraction (λ = 0.2333 Å, 53.14 keV). This method allows penetration of a Teflon-lined stainless steel reaction vessel to measure high-resolution powder patterns at 60 s intervals from which temporal evolution of lattice parameters and Bragg peak area can be refined. Crystallisation in N,N-dimethylformamide (DMF)...
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- Publication status:
- Published
- Peer review status:
- Peer reviewed
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- Files:
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(Accepted manuscript, pdf, 688.5KB)
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- Publisher copy:
- 10.1016/j.micromeso.2017.04.043
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Funding
Bibliographic Details
- Publisher:
- Elsevier Publisher's website
- Journal:
- Microporous and Mesoporous Materials Journal website
- Volume:
- 254
- Pages:
- 178-183
- Publication date:
- 2017-04-22
- Acceptance date:
- 2017-04-19
- DOI:
- ISSN:
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1387-1811
- Source identifiers:
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696609
Item Description
- Keywords:
- Pubs id:
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pubs:696609
- UUID:
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uuid:42328647-21ed-47f6-a921-4f1a99f9643b
- Local pid:
- pubs:696609
- Deposit date:
- 2017-08-16
Terms of use
- Copyright holder:
- © 2017 Elsevier Inc All rights reserved
- Copyright date:
- 2017
- Notes:
- This is the author accepted manuscript following peer review version of the article. The final version is available online from Elsevier at: 10.1016/j.micromeso.2017.04.043
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